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Fulltext Predicting fatigue and damaged modes due to defects of bio-composite materials

Suriania, M.J., Alib, A., Khalina, A., Sapuan, S. M.

Journal of Advanced Research Design, 2015;9(1):1-12.
MyJurnal

In this study, fatigue failures of bio-composite materials were predicted due to
manufacturing defects. Kenaf bast fibres were used to fabricate a bio-composite material with epoxy as
a binding material. The bio-composites were manufactured by using a hand lay-up process. The defects
in the Kenaf/epoxy bio-composite were determined by a non-destructive technique using Infrared
thermal imager. Besides, the thermography analyses were verified via optical microscope and scanning
electron microscope (SEM) investigations. Determinations of fatigue, as well as damage had been
predicted, and it was found that the damage could be fixed with the predicted results.
Fulltext Acute Disseminated Encephalomyelitis (ADEM) Presenting with Bilateral Optic Neuritis

Sapuan S, Basri H

Malays J Med Sci, 2007 Jan;14(1):71-4.
PMID: 22593657 MyJurnal

A 43-year old lady presented with progressive loss of vision in both eyes followed by rapid deterioration of consciousness within the next few days. This was preceded by a viral infection one week before her presentation. At presentation she had evidence of meningism and signs of bilateral upper motor neuron lesions and was managed initially as acute meningoencephalitis with antibiotics. The brain CT was within normal limits but subsequent MRI of the brain revealed multiple foci of hyperintense lesions on T2-weighted and FLAIR images. The cerebrospinal fluid examination revealed lymphocytosis, and normal protein and glucose levels. Cultures of the CSF were negative. She was managed as acute disseminated encephalomyelitis (ADEM) with high-dose of intravenous methlyprednisolone one gram/day for three consecutive days followed by oral prednisolone 60 mg/day. Despite the management she lapsed into coma and succumbed to her illness nine days after admission.
Development of expert system for biobased polymer material selection: food packaging application

Sanyang ML, Sapuan SM

J Food Sci Technol, 2015 Oct;52(10):6445-54.
PMID: 26396389 DOI: 10.1007/s13197-015-1759-6

Biobased food packaging materials are gaining more attention owing to their intrinsic biodegradable nature and renewability. Selection of suitable biobased polymers for food packaging applications could be a tedious task with potential mistakes in choosing the best materials. In this paper, an expert system was developed using Exsys Corvid software to select suitable biobased polymer materials for packaging fruits, dry food and dairy products. If - Then rule based system was utilized to accomplish the material selection process whereas a score system was formulated to facilitate the ranking of selected materials. The expert system selected materials that satisfied all constraints and selection results were presented in suitability sequence depending on their scores. The expert system selected polylactic acid (PLA) as the most suitable material.
Fulltext Effect of glycerol plasticizer loading on the physical, mechanical, thermal, and barrier properties of arrowroot (Maranta arundinacea) starch biopolymers

Tarique J, Sapuan SM, Khalina A

Sci Rep, 2021 07 06;11(1):13900.
PMID: 34230523 DOI: 10.1038/s41598-021-93094-y

This research was set out to explore the development of arrowroot starch (AS) films using glycerol (G) as plasticizer at the ratio of 15, 30, and 45% (w/w, starch basis) using solution casting technique. The developed films were analyzed in terms of physical, structural, mechanical, thermal, environmental, and barrier properties. The incorporation of glycerol to AS film-making solution reduced the brittleness and fragility of films. An increment in glycerol concentration caused an increment in film thickness, moisture content, and solubility in water, whereas density and water absorption were reduced. The tensile strength and modulus of G-plasticized AS films were reduced significantly from 9.34 to 1.95 MPa and 620.79 to 36.08 MPa, respectively, while elongation at break was enhanced from 2.41 to 57.33%. FTIR analysis revealed that intermolecular hydrogen bonding occurred between glycerol and AS in plasticized films compared to control films. The G-plasticized films showed higher thermal stability than control films. The cross-sectional micrographs revealed that the films containing 45% glycerol concentration had higher homogeneity than 15% and 30%. Water vapour permeability of plasticized films increased by an increase in glycerol concentrations. The findings of this research provide insights into the development of bio-degradable food packaging.
The Preparation Methods and Processing of Natural Fibre Bio-polymer Composites

Ilyas RA, Sapuan SM

Curr Org Synth, 2019;16(8):1068-1070.
PMID: 31984916 DOI: 10.2174/157017941608200120105616
Fulltext Mechanical, Physical and Thermal Properties of Sugar Palm Nanocellulose Reinforced Thermoplastic Starch (TPS)/Poly (Lactic Acid) (PLA) Blend Bionanocomposites

Nazrin A, Sapuan SM, Zuhri MYM

Polymers (Basel), 2020 Sep 27;12(10).
PMID: 32992514 DOI: 10.3390/polym12102216

In this paper, sugar palm nanocellulose fibre-reinforced thermoplastic starch (TPS)/poly (lactic acid) (PLA) blend bionanocomposites were prepared using melt blending and compression moulding with different TPS concentrations (20%, 30%, 40%, 60%, and 80%) and constant sugar palm nanocellulose fibres (0.5%). The physical, mechanical, thermal, and water barrier properties were investigated. The SEM images indicated different TPS loading effects with the morphology of the blend bionanocomposites due to their immiscibility. A high content of TPS led to agglomeration, while a lower content resulted in the presence of cracks and voids. The 20% TPS loading reduced the tensile strength from 49.08 to 19.45 MPa and flexural strength from 79.60 to 35.38 MPa. The thermal stability of the blend bionanocomposites was reduced as the TPS loading increased. The thickness swelling, which corresponded to the water absorption, demonstrated an increasing trend with the increased addition of TPS loading.
Fulltext Factors Associated with Good Seizure Control in Patients on Valproic Acid

Ahmad M, Rahman AFA, Sapuan S

Eurasian J Med, 2020 Feb;52(1):41-46.
PMID: 32158313 DOI: 10.5152/eurasianjmed.2020.19039

Objective: This study aims to generate a reference range for valproic acid (VPA) in this cohort and determine the factors associated with good seizure control in patients taking this drug.
Materials and Methods: We conducted a prospective, cohort, observational study among patients with epilepsy who received VPA treatment at Hospital Kuala Lumpur. The patients were considered to have good control if they had a 50% or higher seizure reduction in the one-year study period compared with the previous year. The VPA reference range was generated from those patients who had good control and whose drug concentration values were available. Multiple logistic regression analysis with a backward likelihood ratio method was applied to assess the predicting factors for good seizure control.
Results: A total of 242 patients were recruited and followed up for one year. The VPA reference range was determined to be 40-85 mg/L. After multivariate analysis, significant predictive variables for good control were monotherapy [adjusted OR 4.74, 95% CI: 2.258, 9.947, p<0.001], non-smoking [adjusted OR 3.23, 95% CI: 1.099, 9.473, p=0.033], normal brain imaging results [adjusted OR 5.83, 95% CI: 2.507, 13.552, p<0.001], and the absence of stress [adjusted OR 19.98, 95% CI: 9.255, 42.764, p<0.001].
Conclusion: Monotherapy, non-smoking, normal brain imaging results, and the absence of stress are predictive of good seizure control in patients on VPA. However, a serum concentration of VPA in the reference range failed to predict good seizure control.
Isolation and characterization of nanocrystalline cellulose from sugar palm fibres (Arenga Pinnata)

Ilyas RA, Sapuan SM, Ishak MR

Carbohydr Polym, 2018 Feb 01;181:1038-1051.
PMID: 29253930 DOI: 10.1016/j.carbpol.2017.11.045

Cellulose was extracted from sugar palm fibres (Arenga pinnata) by conducting delignification and mercerization treatments. Subsequently, sugar palm nanocrystalline celluloses (SPNCCs) were isolated from the extracted cellulose with 60wt% concentrated sulphuric acid. The chemical composition of sugar palm fibres were determined at different stages of treatment. Structural analysis was carried out by Brunauer-Emmett-Teller (BET), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR). Morphological analysis of extracted cellulose and isolated nanocrystalline cellulose (NCCs) was investigated by using field emission scanning electron microscopy (FESEM), atomic force microscopy (AFM), and transmission electron microscopy (TEM). The thermal stability of sugar palm fibres at different stages of treatment was investigated by thermogravimetric analysis (TGA). The results showed that lignin and hemicellulose were removed from the extracted cellulose through the delignification and mercerization process, respectively. The isolated SPNCCs were found to have length and diameters of 130±30nm and 9±1.96nm, respectively.
Thermo-mechanical behaviors of thermoplastic starch derived from sugar palm tree (Arenga pinnata)

Sahari J, Sapuan SM, Zainudin ES, Maleque MA

Carbohydr Polym, 2013 Feb 15;92(2):1711-6.
PMID: 23399210 DOI: 10.1016/j.carbpol.2012.11.031

In recent years, increasing environmental concerns focused greater attention on the development of biodegradable materials. A thermoplastic starch derived from bioresources, sugar palm tree was successfully developed in the presence of biodegradable glycerol as a plasticizer. Sugar palm starch (SPS) was added with 15-40 w/w% of glycerol to prepare workable bioplastics and coded as SPS/G15, SPS/G20, SPS/G30 and SPS/G40. The samples were characterized for thermal properties, mechanical properties and moisture absorption on exposure to humidity were evaluated. Morphological studies through scanning electron microscopy (SEM) were used to explain the observed mechanical properties. Generally, the addition of glycerol decrease the transition temperature of plasticized SPS. The mechanical properties of plasticized SPS increase with the increasing of glycerol but up to 30 w/w%. Meanwhile, the water absorption of plasticized SPS decrease with increasing of glycerol.
Development and characterization of sugar palm starch and poly(lactic acid) bilayer films

Sanyang ML, Sapuan SM, Jawaid M, Ishak MR, Sahari J

Carbohydr Polym, 2016 08 01;146:36-45.
PMID: 27112848 DOI: 10.1016/j.carbpol.2016.03.051

The development and characterization of environmentally friendly bilayer films from sugar palm starch (SPS) and poly(lactic acid) (PLA) were conducted in this study. The SPS-PLA bilayer films and their individual components were characterized for their physical, mechanical, thermal and water barrier properties. Addition of 50% PLA layer onto 50% SPS layer (SPS50-PLA50) increased the tensile strength of neat SPS film from 7.74 to 13.65MPa but reduced their elongation at break from 46.66 to 15.53%. The incorporation of PLA layer significantly reduced the water vapor permeability as well as the water uptake and solubility of bilayer films which was attributed to the hydrophobic characteristic of the PLA layer. Furthermore, scanning electron microscopy (SEM) image of SPS50-PLA50 revealed lack of strong interfacial adhesion between the SPS and PLA. Overall, the incorporation of PLA layer onto SPS films enhances the suitability of SPS based films for food packaging.
Characteristics of thermoplastic sugar palm Starch/Agar blend: Thermal, tensile, and physical properties

Jumaidin R, Sapuan SM, Jawaid M, Ishak MR, Sahari J

Int J Biol Macromol, 2016 Aug;89:575-81.
PMID: 27177458 DOI: 10.1016/j.ijbiomac.2016.05.028

The aim of this work is to study the behavior of biodegradable sugar palm starch (SPS) based thermoplastic containing agar in the range of 10-40wt%. The thermoplastics were melt-mixed and then hot pressed at 140°C for 10min. SEM investigation showed good miscibility between SPS and agar. FT-IR analysis confirmed that SPS and agar were compatible and inter-molecular hydrogen bonds existed between them. Incorporation of agar increased the thermoplastic starch tensile properties (Young's modulus and tensile strength). The thermal stability and moisture uptake increased with increasing agar content. The present work shows that starch-based thermoplastics with 30wt% agar content have the highest tensile strength. Higher content of agar (40wt%) resulted to more rough cleavage fracture and slight decrease in the tensile strength. In conclusion, the addition of agar improved the thermal and tensile properties of thermoplastic SPS which widened the potential application of this eco-friendly material. The most promising applications for this eco-friendly material are short-life products such as packaging, container, tray, etc.
Effect of plasticizer type and concentration on physical properties of biodegradable films based on sugar palm (arenga pinnata) starch for food packaging

Sanyang ML, Sapuan SM, Jawaid M, Ishak MR, Sahari J

J Food Sci Technol, 2016 Jan;53(1):326-36.
PMID: 26787952 DOI: 10.1007/s13197-015-2009-7

In this study, sugar palm starch (SPS) films were developed using glycerol (G), sorbitol (S) or their combination (GS) as plasticizers at the ratio of 15, 30 and 45 (wt)% using casting technique. The addition of plasticizers to SPS film-forming solutions helped to overcome the brittle and fragile nature of unplasticized SPS films. Increased plasticizer concentration resulted to an increase in film thickness, moisture content and solubility. On the contrary, density and water absorption of plasticized films decreased with increasing plasticizer concentration. Raising the plasticizer content from 15 to 45 % showed less effect on the moisture content and water absorption of S-plasticized films. Films containing glycerol and glycerol-sorbitol plasticizer (G, and GS) demonstrated higher moisture content, solubility and water absorption capacity compared to S-plasticized films. The results obtained in this study showed that plasticizer type and concentration significantly improves film properties and enhances their suitability for food packaging applications.
Potential of using multiscale corn husk fiber as reinforcing filler in cornstarch-based biocomposites

Ibrahim MIJ, Sapuan SM, Zainudin ES, Zuhri MYM

Int J Biol Macromol, 2019 Oct 15;139:596-604.
PMID: 31381916 DOI: 10.1016/j.ijbiomac.2019.08.015

In this study, biodegradable composite films were prepared by using thermoplastic cornstarch matrix and corn husk fiber as a reinforcing filler. The composite films were manufactured via a casting technique using different concentrations of husk fiber (0-8%), and fructose as a plasticizer at a fixed amount of 25% for starch weight. The Physical, thermal, morphological, and tensile characteristics of composite films were investigated. The findings indicated that the incorporation of husk fiber, in general, enhanced the performance of the composite films. There was a noticeable reduction in the density and moisture content of the films, and soil burial assessment showed less resistance to biodegradation. The morphological images presented a consistent structure and excellent compatibility between matrix and reinforcement, which reflected on the improved tensile strength and young modulus as well as the crystallinity index. The thermal stability of composite films has also been enhanced, as evidenced by the increased onset decomposition temperature of the reinforced films compared to neat film. Fourier transform infrared analysis revealed increasing in intermolecular hydrogen bonding following fiber loading. The composite materials prepared using corn husk residues as reinforcement responded to community demand for agricultural and polymeric waste disposal and added more value to waste management.
Fulltext Extraction and Characterization of Potential Biodegradable Materials Based on Dioscorea hispida Tubers

Hazrati KZ, Sapuan SM, Zuhri MYM, Jumaidin R

Polymers (Basel), 2021 Feb 15;13(4).
PMID: 33672030 DOI: 10.3390/polym13040584

This study was driven by the stringent environmental legislation concerning the consumption and utilization of eco-friendly materials. Within this context, this paper aimed to examine the characteristics of starch and fibres from the Dioscorea hispida tuber plant to explore their potential as renewable materials. The extraction of the Dioscorea hispida starch and Dioscorea hispida fibres was carried out and the chemical composition, physical, thermal, morphological properties, and crystallinity were studied. The chemical composition investigations revealed that the Dioscorea hispida starch (DHS) has a low moisture t (9.45%) and starch content (37.62%) compared to cassava, corn, sugar palm, and arrowroot starches. Meanwhile, the Dioscorea hispida fibres (DHF) are significantly low in hemicellulose (4.36%), cellulose (5.63%), and lignin (2.79%) compared to cassava, corn hull and sugar palm. In this investigation the chemical, physical, morphological and thermal properties of the Dioscorea hispida fibre and Dioscorea hispida starch were examined by chemical composition investigation, scanning electron microscopy (SEM), particle size distribution, thermogravimetric analysis (TGA), X-ray powder diffraction (XRD), and Fourier transform infrared (FTIR), respectively. It was found that Dioscorea hispida waste is promising alternative biomass and sustainable material with excellent potential as a renewable filler material for food packaging applications.
Fulltext Experimental Analysis of Heat-Affected Zone (HAZ) in Laser Cutting of Sugar Palm Fiber Reinforced Unsaturated Polyester Composites

Masoud F, Sapuan SM, Ariffin MKAM, Nukman Y, Bayraktar E

Polymers (Basel), 2021 Feb 26;13(5).
PMID: 33652612 DOI: 10.3390/polym13050706

In this paper, the influence of processing input parameters on the heat-affected zone (HAZ) of three different material thicknesses of sugar palm fiber reinforced unsaturated polyester (SPF-UPE) composites cut with a CO2 laser was investigated. Laser power, traverse speed, and gas pressure were selected as the most influential input parameters on the HAZ to optimize the HAZ response with fixing all of the other input parameters. Taguchi's method was used to determine the levels of parameters that give the best response to the HAZ. The significance of input parameters was also determined by calculating the max-min variance of the average of the signal-to-noise ratio (S/N) ratio for each parameter. Analysis of variation (ANOVA) was used to determine each input parameter's contribution to the influence on HAZ depth. The general results show that the minimum levels of laser power and the highest levels of traverse speed and gas pressure gave the optimum response to the HAZ. Gas pressure had the most significant effect on the HAZ, with contribution decreases as the material thickness increased, followed by the traverse speed with contribution increases with the increase in material thickness. Laser power came third, with a minimal contribution to the effect on the HAZ, and it did not show a clear relationship with the change in material thickness. By applying the optimum parameters, the desired HAZ depth could be obtained at relatively low values.
Fulltext Experimental Analysis of Kerf Taper Angle in Cutting Process of Sugar Palm Fiber Reinforced Unsaturated Polyester Composites with Laser Beam and Abrasive Water Jet Cutting Technologies

Masoud F, Sapuan SM, Ariffin MKAM, Nukman Y, Bayraktar E

Polymers (Basel), 2021 Jul 31;13(15).
PMID: 34372145 DOI: 10.3390/polym13152543

In this research, the effect of processing input parameters on the kerf taper angle response of three various material thicknesses of sugar palm fiber reinforced unsaturated polyester composite was investigated as an output parameter from abrasive waterjet and laser beam cutting techniques. The main purpose of the study is to obtain data that includes the optimum input parameters in cutting the composite utilizing these two unconventional techniques to avoid some defects that arise when using traditional cutting methods for cutting the composites, and then make a comparison to determine which is the most appropriate technique regarding the kerf taper angle response that is desired to be reduced. In the laser beam cutting process, traverse speed, laser power, and assist gas pressure were selected as the variable input parameters to optimize the kerf taper angle. While the water pressure, traverse speed, and stand-off-distance were the input variable parameters in the case of waterjet cutting process, with fixing of all the other input parameters in both cutting techniques. The levels of the input parameters that provide the optimal response of the kerf taper angle were determined using Taguchi's approach, and the significance of input parameters was determined by computing the max-min variance of the average of the signal to-noise ratio (S/N) for each parameter. The contribution of each input processing parameter to the effects on kerf taper angle was determined using analysis of variation (ANOVA). Compared with the results that were extrapolated in the previous studies, both processes achieved acceptable results in terms of the response of the kerf taper angle, noting that the average values produced from the laser cutting process are much lower than those resulting from the waterjet cutting process, which gives an advantage to the laser cutting technique.
Effect of plasticizers on physical, thermal, and tensile properties of thermoplastic films based on Dioscorea hispida starch

Hazrati KZ, Sapuan SM, Zuhri MYM, Jumaidin R

Int J Biol Macromol, 2021 Aug 31;185:219-228.
PMID: 34153358 DOI: 10.1016/j.ijbiomac.2021.06.099

This study examines the effects of varying the concentrations of sorbitol (S) and glycerol (G) on the physical, morphological, thermal, and mechanical properties of Dioscorea hispida, starch-based films. In this context, the films of Dioscorea hispida starch were developed using solution casting technique with glycerol (G), sorbitol (S), and a mixture of sorbitol-glycerol (SG) as plasticizers at the ratios of 0, 30, 45, and 60 wt%. The films' moisture contents were increased when increasing the plasticizer contents. The tensile strengths were decreased, but elongations at break were increased; 7.38%-11.54% for G-plasticized films, 10.17%-15.76% for S-plasticized films, and 14.41%- 16.10% for SG-plasticized films with increasing plasticizer concentrations of the film samples. Varying plasticizer concentrations exhibited a minor effect on the S-plasticized film's thermal properties. Significant decrement in the glass transition temperatures of Dioscorea hispida starch films was observed when the plasticizer contents were raised from 30% to 60%. Significantly, the present work has shown that plasticized Dioscorea hispida starch can be considered a promising biopolymer for the applications of biodegradable films.
Fulltext Development and Characterization of Polypropylene Waste from Personal Protective Equipment (PPE)-Derived Char-Filled Sugar Palm Starch Biocomposite Briquettes

Harussani MM, Sapuan SM, Rashid U, Khalina A

Polymers (Basel), 2021 May 24;13(11).
PMID: 34073691 DOI: 10.3390/polym13111707

Slow pyrolysis using a batch reactor at 450 °C was applied to the polypropylene (PP) powder derived from Coronavirus Disease 2019 (COVID-19) isolation gown waste to yield char briquettes, using sugar palm starch (SPS) and a manual hydraulic press. These studies are significant because of reductions in plastic waste from the preparation of barbecue coal due to environmental sustainability. The results presented here include the physical, morphological, thermal, combustion, and mechanical properties of char when reinforced with various percentages of SPS loadings (0, 10, 20, 30, and 40%), which act as a matrix/binder to produce char/sugar palm starch (C/SPS) composites. The physical and morphological characteristics of C/SPS composites were determined using Fourier transform infrared (FTIR) and field emission scanning electron microscopy (FESEM). On the other hand, the thermal and combustion properties of the C/SPS briquettes were studied via thermogravimetric and bomb calorimeter analysis. The results show that the compressive strength of the briquettes increased as the SPS loading increased, whereas the higher heating values (HHV) reduced. The findings indicate that C-80/SPS-20 briquettes presented excellent combustion characteristics (1,761,430 J/g) with satisfactory mechanical strength (1.463 MPa) in the compression test. Thus, C-80/SPS-20 briquettes are the most suitable composites for domestic and commercial uses.
Fulltext Thermal Stability and Dynamic Mechanical Analysis of Benzoylation Treated Sugar Palm/Kenaf Fiber Reinforced Polypropylene Hybrid Composites

Mohd Izwan S, Sapuan SM, Zuhri MYM, Mohamed AR

Polymers (Basel), 2021 Aug 31;13(17).
PMID: 34503001 DOI: 10.3390/polym13172961

This research was performed to evaluate the mechanical and thermal properties of sugar palm fiber (SPF)- and kenaf fiber (KF)-reinforced polypropylene (PP) composites. Sugar palm/kenaf was successfully treated by benzoylation treatment. The hybridized bio-composites (PP/SPF/KF) were fabricated with overall 10 weight percentage (wt%) relatively with three different fibers ratios between sugar palm-treated and kenaf-treated (7:3, 5:5, 3:7) and vice versa. The investigations of thermal stability were then carried out by using diffraction scanning calorimetry (DSC) and thermogravimetry analysis (TGA). The result of a flammability test showed that the treated hybrid composite (PP/SPF/KF) was the specimen that exhibited the best flammability properties, having the lowest average burning rate of 28 mm/min. The stiffness storage modulus (E'), loss modulus (E"), and damping factor (Tan δ) were examined by using dynamic mechanical analysis (DMA). The hybrid composite with the best ratio (PP/SPF/KF), T-SP5K5, showed a loss modulus (E") of 86.2 MPa and a damping factor of 0.058. In addition, thermomechanical analysis (TMA) of the studies of the dimension coefficient (µm) against temperature were successfully recorded, with T-SP5K5 achieving the highest dimensional coefficient of 30.11 µm at 105 °C.
Melt volume flow rate and melt flow rate of kenaf fibre reinforced Floreon/magnesium hydroxide biocomposites

Lee CH, Sapuan SM, Lee JH, Hassan MR

Springerplus, 2016;5(1):1680.
PMID: 27733982

A study of the melt volume flow rate (MVR) and the melt flow rate (MFR) of kenaf fibre (KF) reinforced Floreon (FLO) and magnesium hydroxide (MH) biocomposites under different temperatures (160-180 °C) and weight loadings (2.16, 5, 10 kg) is presented in this paper. FLO has the lowest values of MFR and MVR. The increment of the melt flow properties (MVR and MFR) has been found for KF or MH insertion due to the hydrolytic degradation of the polylactic acid in FLO. Deterioration of the entanglement density at high temperature, shear thinning and wall slip velocity were the possible causes for the higher melt flow properties. Increasing the KF loadings caused the higher melt flow properties while the higher MH contents created stronger bonding for higher macromolecular chain flow resistance, hence lower melt flow properties were recorded. However, the complicated melt flow behaviour of the KF reinforced FLO/MH biocomposites was found in this study. The high probability of KF-KF and KF-MH collisions was expected and there were more collisions for higher fibre and filler loading causing lower melt flow properties.

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