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Mechanical, morphological and structural properties of cellulose nanofibers reinforced epoxy composites

Saba N, Mohammad F, Pervaiz M, Jawaid M, Alothman OY, Sain M

Int J Biol Macromol, 2017 Apr;97:190-200.
PMID: 28082223 DOI: 10.1016/j.ijbiomac.2017.01.029

Present study, deals about isolation and characterization of cellulose nanofibers (CNFs) from the Northern Bleached Softwood Kraft (NBSK) pulp, fabrication by hand lay-up technique and characterization of fabricated epoxy nanocomposites at different filler loadings (0.5%, 0.75%, 1% by wt.). The effect of CNFs loading on mechanical (tensile, impact and flexural), morphological (scanning electron microscope and transmission electron microscope) and structural (XRD and FTIR) properties of epoxy composites were investigated. FTIR analysis confirms the introduction of CNFs into the epoxy matrix while no considerable change in the crystallinity and diffraction peaks of epoxy composites were observed by the XRD patterns. Additions of CNFs considerably enhance the mechanical properties of epoxy composites but a remarkable improvement is observed for 0.75% CNFs as compared to the rest epoxy nanocomposites. In addition, the electron micrographs revealed the perfect distribution and dispersion of CNFs in the epoxy matrix for the 0.75% CNFs/epoxy nanocomposites, while the existence of voids and agglomerations were observed beyond 0.75% CNFs filler loadings. Overall results analysis clearly revealed that the 0.75% CNFs filler loading is best and effective with respect to rest to enhance the mechanical and structural properties of the epoxy composites.
Fulltext Outpatient Percutaneous Release of Trigger Finger: A Cost Effective and Safe Procedure

Marij Z, Aurangzeb Q, Rizwan HR, Haroon R, Pervaiz MH

Malays Orthop J, 2017 Mar;11(1):52-56.
PMID: 28435575 DOI: 10.5704/MOJ.1703.021

INTRODUCTION: Trigger finger is a common cause of pain and disability of the hand. Percutaneous release results in earlier functional recovery and patient satisfaction. This is a rapid and cost-effective method which saves a surgical procedure and results in better functional outcome.
MATERIALS AND METHODS: This is a prospective observational study conducted on fifty-two fingers and thumbs in 52 patients treated from 1st July 2014 till 31st December 2014, in the Orthopaedic Section, Department of Surgery, Aga Khan University Hospital, Karachi, Pakistan. All the baseline characteristics of the patients, like demographics, symptoms, Quinell's criteria and functional outcome were recorded. The patients were treated at our hospital with trigger finger, managed with percutaneous release using an 18 gauge needle and followed up for a minimum period of three months. The follow-up information included range of motion scoring, patient satisfaction and overall outcome of the procedure in terms of patient acceptance. The data was analyzed to determine the functional outcome at three months.
RESULTS: There was complete release of A1 pulleys in 52 out of 52 digits (100%) in the patients undergoing percutaneous release and significant patient satisfaction. No recurrence was observed.
CONCLUSION: Percutaneous release of trigger finger with needle was not only associated with excellent functional outcome and recovery in terms of patient satisfaction and range of finger motion three months post-procedure but also was found to be cost effective.
Thermal and dynamic mechanical properties of cellulose nanofibers reinforced epoxy composites

Saba N, Safwan A, Sanyang ML, Mohammad F, Pervaiz M, Jawaid M, et al.

Int J Biol Macromol, 2017 Sep;102:822-828.
PMID: 28455253 DOI: 10.1016/j.ijbiomac.2017.04.074

The current study presents about the effect of cellulose nanofibers (CNFs) filler on the thermal and dynamic mechanical analysis (DMA) of epoxy composites as a function of temperature. In this study hand lay-up method was used to fabricate CNF reinforced Epoxy nanocomposites with CNF loading of 0.5%, 0.75%, and 1% into epoxy resin. The obtained thermal and DMA results illustrates that thermal stability, char content, storage modulus (E'), loss modulus (E") and glass transition temperature (Tg) increases for all CNF/epoxy nanocomposites compared to the pure epoxy. Thermal results revealed that 0.75% offers superior resistance or stability towards heat compared to its counterparts. In addition, 0.75% CNF/epoxy nanocomposites confers highest value of storage modulus as compared to 0.5% and 1% filler loading. Hence, it is concluded that 0.75% CNFs loading is the minimal to enhance both thermal and dynamic mechanical properties of the epoxy composites and can be utilized for advance material applications where thermal stability along with renewability are prime requirements.

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